Assessment of the feasibility of determining the volume fraction and characteristics of the size, shape and distribution of γ’ phase precipitates in nickel-based superalloys
Assessment of the feasibility of determining the volume fraction and characteristics of the size, shape and distribution of γ’ phase precipitates in nickel-based superalloys
Assessment of the feasibility of determining the volume fraction and characteristics of the size, shape and distribution of γ’ phase precipitates in nickel-based superalloys
Autor
Szczotok, Agnieszka
Opublikowane w
Technical Transactions
Numeracja
Vol. 120, iss. 1
Data wydania
2023
Miejsce wydania
Warsaw
Wydawca
Sciendo
Sekcja czasopisma
Mechanics
Język
angielski
eISSN
2353-737X
DOI
https://doi.org/10.37705/TechTrans/e2023011
Słowa kluczowe
volume fraction, size, shape, distribution, γ' phase precipitates, Ni-basedsuperalloys, research methods
Abstrakt
This overview presents a comprehensive exploration of the research methodsemployed for the precise assessment of volume fraction and the detailedcharacterisation of the size, shape and distribution of γ' phase precipitates withinNi-based superalloys. These advanced materials exhibit exceptional mechanicalproperties due to the presence of γ' precipitates. The accurate quantification ofprecipitate parameters is crucial for understanding material behaviour and forthe optimisation of alloy design. In this overview, a spectrum of techniques,including microscopy (SEM, TEM), diffraction (XRD), spectroscopy (EDS, EELS)and advanced imaging (3D-APT, STEM-HAADF, FIB-SEM) is discussed. Strengths,limitations and potential synergies among these methods are highlighted, offeringresearchers a comprehensive toolbox to advance their investigations of γ' phaseprecipitates in Ni-based superalloys.